SOP FOR PREPARATION AND STANDARDIZATION OF 0.01M LEAD NITRATE

PREPARATION:
Dissolve 3.312 g of Lead nitrate in sufficient water to produce 1000 ml.
STANDARISATION:
Piptte 50 ml of the solution into a flask,add 50 mg of xylenol orange mixture and sufficient hexamine to produce a violet pink colour and titrate with 0.1 M disodium edetate to a lemon yellow end point.
Each ml of 0.1M disodium edetate is equivalent to 0.03312 g of Lead nitrate
Molarity factor : 0.03312 x 50 x V/1000 X W
Where
V = Volume of 0.1M disodium edetate consumed in ml.
W = Weight of lead nitrate in g
Note:
1) Restandardise before use.
2) Discard the solution after 30 days.
3) For storage and labeling follow the general procedure.